Vacuum FTIR Vertex70v + microscope Hyperion 3000 KIT - polarizors (FTIR)

Vacuum FTIR Vertex70v + microscope Hyperion 3000 KIT - polarizors
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Guarantor: Alois Nebojsa
Technology / Methodology: Optical measurements
Instrument status: Some Issues Some Issues, 12.4.2024 12:10, The beamsplitter door is blocked. There is a KBR beamsplitter in the interferometer (MIR range) Repair on April 18
Research group: CF: CEITEC Nano


Description:

Instrument consists of a combination of Fourier infrared spectrometer with infrared microscope. In the spectrometer, one can perform transmission and reflection experiments on samples dimension of roughly 1 mm2 and more in the full frequency range offered by the spectrometer, 30-14 000 cm-1. The microscope is used for measurements of either small or spatially inhomogeneous samples essentially down to the diffraction limit in the far field, it means roughly 3 at 3000 cm-1. The frequency range is however limited by the microscope detectors to 600-6000 cm-1. The highlight of this microscope is the focal plane array (FPA) detector that allows simultaneous recording of 128x128 matrix of spectra in the frequency range 900-5000 cm-1.


Publications:

  • Chennam, P. K.; Kachlík, M.; Říhová, M.; Čičmancová, V.; Maca, K.; Macak, J. M., 2024: Synthesis of centrifugally spun polyacrylonitrile-carbon fibers. JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY 28, p. 2199 - 2205, doi: 10.1016/j.jmrt.2023.12.146; FULL TEXT
    (RIGAKU3, WITEC-RAMAN, VERIOS, LEICACOAT-STAN, FTIR)
  • Kelarová, Š., 2023: Organosilicon coatings based on trimethylsilyl acetate monomer prepared using plasma of RF capacitively coupled glow discharge. PH.D. THESIS , p. 1 - 182; FULL TEXT
    (WOOLLAM-MIR, FTIR, KRATOS-XPS, SIMS)
  • TINOCO NAVARRO, L.; CIHLÁŘ, J.; MICHALIČKA, J.; KAŠTYL, J.; ČÁSTKOVÁ, K., 2023: Effect of MCAA Synthesis and Calcination Temperature on Heterojunction Formation and Photocatalytic Activity of Biphasic TiO2 (B/A). CATALYSIS LETTERS 2, doi: 10.1007/s10562-023-04489-7; FULL TEXT
    (RIGAKU3, WITEC-RAMAN, FTIR, VERIOS, TITAN, KRATOS-XPS, BET-DEGASSER, BET-ANAMET, ZETASIZER)
  • ORUDZEV, F.; SELIMOV, D.; RABADANOVA, A.; SHUAIBOV, A.; ABDURAKHAMANOV, M;. GULAKHMEDOV, R.; PAPEZ, N.; SHIKHGASAN, R.; ZVEREVA, I.; CASTKOVA, K., 2023: 1D/2D Electrospun Polyvinylidene Fluoride Nanofibers/Carbon Flakes Hybrid Nonmetal Polymeric Photo- and Piezocatalyst. CHEMISTRYSELECT 8(43), p. 1 - 11, doi: 10.1002/slct.202303318; FULL TEXT
    (WITEC-RAMAN, KRATOS-XPS, VERIOS, LEICACOAT-STAN, FTIR, RIGAKU3)
  • PALACIOS CORELLA, M.; ROJAS TIZÓN, J.; PUMERA, M., 2023: Photocatalytic Pt/Ag3VO4 micromotors with inherent sensing capabilities for corroding environments. JOURNAL OF COLLOID AND INTERFACE SCIENCE 631, p. 125 - 10, doi: 10.1016/j.jcis.2022.10.169; FULL TEXT
    (KRATOS-XPS, FTIR, RIGAKU3, LYRA)

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